Effects of processing high amylose maize starches under controlled conditions on structural organisation and amylase digestibility

A. Htoon, A. K. Shrestha, B. M. Flanagan, A. Lopez-Rubio, A. R. Bird, E. P. Gilbert, M. J. Gidley

    Research output: Contribution to journalArticlepeer-review

    Abstract

    The amylase digestibility of high-amylose maize starches has been compared before and after thermo-mechanical processing. Starches were analysed for enzyme-resistant starch yield, apparent amylose content, crystallinity (X-ray diffraction), and molecular order (NMR and FTIR), both before and after treatment with α-amylase. All samples had significant (>10%) enzyme-resistant starch levels irrespective of the type and extent of thermal or enzymic processing. Molecular or crystalline order was not a pre-requisite for enzyme resistance. Near-amorphous forms of high amylose maize starches are likely to undergo recrystallisation during the enzyme-digestion process. The mechanism of enzyme resistance of granular high-amylose starches is found to be qualitatively different to that for processed high-amylose starches. For all samples, measured levels of enzyme resistance are due to the interruption of a slow digestion process, rather than the presence of completely indigestible material.
    Original languageEnglish
    Pages (from-to)236-245
    Number of pages10
    JournalCarbohydrate Polymers
    Volume75
    Issue number2
    DOIs
    Publication statusPublished - 2009

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