Enhanced photocatalytic activity of (La, N) co-doped TiO2 by TiCl4 sol-gel autoigniting synthesis

Zhongqing Liu, Yanping Zhou, Zhenghua Li, Yichao Wang, Changchun Ge

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13 Citations (Scopus)

Abstract

(La, N) co-doped TiO2 photocatalysts were synthesized using TiCl4 sol-gel autoigniting synthesis (SAS) starting from a complex compound system of TiCl4-La(NO3)3-citric acid-NH4NO3-NH3.H2O, in which the (La, N) co-doped process was accomplished in the formation of TiO2 nanocrystals. The prepared samples were characterized by using X-ray diffraction (XRD), X-ray photoemission spectroscopy (XPS) and UV-vis diffuse reflectance spectra. The results indicated that nitrogen and lanthanum were incorporated into the lattice and interstices of titania nanocrystals, which resulted in narrowing the band gap and promoting the separation of photoexcited hole-electron pairs, respectively, and showing expected red-shifts and enhanced photocatalytic activity under visible light. The mechanism on nitrogen doping and enhancement in photocatalytic activity of (La, N) co-doped titania by SAS was discussed in detail.
Original languageEnglish
Pages (from-to)552-557
Number of pages6
JournalJournal of University of Science and Technology Beijing
Volume14
Issue number6
DOIs
Publication statusPublished - 2007

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