Pulsed gradient spin-echo NMR

Gang Zheng, Anwen Krause-Heuer, William S. Price

    Research output: Chapter in Book / Conference PaperChapter

    Abstract

    In this chapter, the fundamentals of translational diffusion and PGSE NMR diffusion measurements and the solutions of the common artefacts in PGSE experiments (such as background gradients, huge solvent (e.g., water) signal, and thermal convection) are discussed and the practical issues of PGSE measurements (including sample preparation, selection of pulse sequences, and parameter settings) are considered; the fundamentals of the application of PGSE NMR to the study of ligand-macromolecule interactions and supramolecular assembly are examined.
    Original languageEnglish
    Title of host publicationMetallointercalators: Synthesis and Techniques to Probe Their Interactions with Biomolecules
    EditorsJanice R. Aldrich-Wright
    Place of PublicationU.S.
    PublisherSpringer
    Pages159-185
    Number of pages27
    ISBN (Electronic)9783211990797
    ISBN (Print)9783211094273
    DOIs
    Publication statusPublished - 2011

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