Pulsed gradient spin-echo NMR

Gang Zheng, Anwen Krause-Heuer, William S. Price

Research output: Chapter in Book / Conference PaperChapter

Abstract

In this chapter, the fundamentals of translational diffusion and PGSE NMR diffusion measurements and the solutions of the common artefacts in PGSE experiments (such as background gradients, huge solvent (e.g., water) signal, and thermal convection) are discussed and the practical issues of PGSE measurements (including sample preparation, selection of pulse sequences, and parameter settings) are considered; the fundamentals of the application of PGSE NMR to the study of ligand-macromolecule interactions and supramolecular assembly are examined.
Original languageEnglish
Title of host publicationMetallointercalators: Synthesis and Techniques to Probe Their Interactions with Biomolecules
EditorsJanice R. Aldrich-Wright
Place of PublicationU.S.
PublisherSpringer
Pages159-185
Number of pages27
ISBN (Electronic)9783211990797
ISBN (Print)9783211094273
DOIs
Publication statusPublished - 2011

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